Metallographic investigation of the diffusion zone of 31CrMoV9 steel after gas nitriding
DOI:
https://doi.org/10.22399/ijcesen.873Keywords:
steel, Nitriding, zone, Diffusion, Metallographic, kineticAbstract
Gas nitriding is a process of thermal treatment of steels, which is carried out at temperatures higher than 5000C. During this process, the peripheral layer of the steel is enriched with nitrogen and thus changes its physical properties. The layer enriched with nitrogen consists of two zones: compound and diffusions or precipitates zone. The thicknesses of the zones depend on nitriding parameters: temperature, duration of nitriding and nitriding parameter. For research we had the chromium-enriched steel 31CrMoV9. Nitriding of this steel was done at three different temperatures 5100C, 5500C and 5900C. For each temperature, there were four different durations of stay of the samples in the furnace where nitriding was performed. Then, the samples were investigated by various experimental methods. In this contribution, we will present the results of metallographic research, namely optical microscopy. With the help of the optical microscope, we found the thicknesses of the diffusions zones from which we calculated the growth kinetics of these zones
References
[1] V Coufal et al. (2023). Comparison of physical, mechanical and chemical properties of barrel steel 32CrMoV12-10 and nitriding steel 31CrMoV9 after nitriding in gas. Phys.: Conf. Ser. 2572 012005. DOI: 10.1088/1742-6596/2572/1/012005.
[2] Nguyen Duong Nam et al. (2019). Control gas nitriding process: a review. Journal of Mechanical Engineering Research & Developments (JMERD) 42(1) 17-25 DOI: 10.26480/jmerd.01.2019.17.25.
[3]Naim Syla, Nazmi Hasi. (2016). Study of the compound layer of gas nitride 31CrMoV9 steel. The 4th Global Virtual Conference DOI: 10.18638/gv.2016.4.1.776.
[4] Zbigniew Gronostajski et al. (2020). Influence of the phase structure of nitrides and properties of nitrided layers on the durability of tools applied in hot forging processes. Journal of Manufacturing Processes 52;247-262 DOI: 10.1016/j.jmapro.2020.01.037.
[5] Zahra eta al. (2024). Exploring microstructural evolution, nitrogen depth profile, and dry wear performance in 31CrMoV9 steel through combined severe shot peening and plasma nitriding. Materials today communications. DOI: 10.1016/j.mtcomm.2024.109182.
[6] H.-J. Spies et al. (1995) Adhesion and wear resistance of nitrided and TiN coated low alloy steels. Surface and Coatings Technology.DOI: 10.1016/0257-8972(95)08366-9.
[7] S. Hoja et al. (2020). Compound Layer Design for Deep Nitrided Gearings. Metals. DOI: 10.3390/met10040455.
[8] Naim Syla et al. (2021). Comparison of Experimental Curves of Alloy Steels after Gas Nitriding. International Journal of Computational and Experimental Science and Engineering. DOI:10.22399/ijcesen.798206.
[9] A Ciski et al. (2017). Heat treatment of nitrided layer formed on X37CrMoV5-1 hot working tool steel. 4th International Conference Recent Trends in Structural Materials. DOI: 10.1088/1757-899X/179/1/012013.
[10] Naim Syla et al. (2008). Experimental Study of the Nitriding Layer by Steel 17CrMoV10. Journal of Engineering and Applied Sciences 3(10).DOI: jeasci.2008.754.757
[11] Enes Akca, Erwin Trgo (2015). Metallographic Procedures and Analysis – A review. Periodicals of engineering and natural sciences 3(2) DOI: 10.21533/pen
[12] Nana Wang, Jinxiang Liu (2013). Effect of Process Parameters on Gas Nitriding of Grey Cast Iron. Advances in Materials Science and Engineering DOI: 10.1155/2013/217848
[13] Yu-Hsuan Lin (2023). Gas Nitriding Behavior of Refractory Metals and Implications for Multi-Principal Element Alloy Design. Journal of Alloys and Compounds.
Downloads
Published
How to Cite
Issue
Section
License
Copyright (c) 2025 International Journal of Computational and Experimental Science and Engineering

This work is licensed under a Creative Commons Attribution 4.0 International License.